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10 Jun 2020 12:18:12 UTC
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Platinum Recovery from Laboratory Chemical Waste (Pt 2)
In this video we recover platinum from platinum containing laboratory chemical waste.

This method was heavily drawn from the method at this citation: G.B. Kauffman, L.A. Teter, Inorg. Synth. 7 (1963) 232–236

Now laboratory chemical waste needs to be incinerated first to remove all organic compounds. Chemical methods are not used because they are more expensive and cannot deal with all types of organic residues. Incineration is the cheapest broadly applicable solution. We've already done this in part 1 of this series: https://www.youtube.com/watch?v=xeKZdJ1As7I

Now in this video we process the platinum concentrate powder into platinum metal. We're using 2.4g of platinum concentrate but your numbers may be adjusted accordingly

First we boil the powder with some concentrated hydrochloric acid. About 10-25ml of acid per gram of platinum concentrate. The mixture is then filtered and the residue is subjected to aqua regia digestion. About 4mL of aqua regia (3ml hcl and 1 mL nitric acid) for every gram of platinum concentrate. The mixture is gently heated to drive the reaction. After all the nitrogen oxides have been driven off the mixture is filtered and is again subjected to aqua regia treatment. This is repeated until the filtrate is a constant shade of light yellow or until stannous chloride testing shows no metals dissolving. The residue is then weighed to determine how much metal was dissolved.

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https://www.youtube.com/watch?v=7B-EwKOqqv4
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